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Synthesis Of 25x-Bomes And 25x-Nbohs (X = H, I, Br) For Pharmacological Studies And As Reference Standards For Forensic Purposes

TETRAHEDRON LETTERS(2021)

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Abstract
An expeditious method is reported for the synthesis of three NBOHs (25H-, 25I- and 25B-NBOH; 9-38% overall yield) and three NBOMes (25H-, 25I- and 25B-NBOMe; 7-33% overall yield) from salicylaldehyde and 2-methoxyaldehyde, respectively. The X-ray structures of 25H-, 25I- and 25B-NBOH center dot HCl were also determined. Our approach should provide a general entry for preparing such a class of substances for pharmacological and forensic purposes. (C) 2021 Elsevier Ltd. All rights reserved.
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Key words
Phenethylamines, Reference standards, NBOMe, NBOH
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