6-Hydroxy-2-Methylbenzofuran-4-Carboxylic Acid

Matteo Mori,Fiorella Meneghetti,Laurent R. Chiarelli, Alessia Diego,Donatella Nava,Arianna Gelain,Giulia Cazzaniga,Stefania Villa,Elena Pini

MOLBANK（2020）

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摘要

6-Hydroxy-2-methylbenzofuran-4-carboxylic acid was synthesized in two steps, starting from 3,5-dihydroxybenzoate. The product was obtained through a direct thermal one-pot cyclization with propargyl bromide, followed by a base-catalyzed hydrolysis. Its molecular structure was elucidated by means of mono- and bidimensional NMR techniques, ESI-MS, FT-IR and single-crystal X-ray diffraction.

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关键词

6-hydroxy-2-methylbenzofuran-4-carboxylic acid methyl ester, 6-hydroxy-2-methylbenzofuran-4-carboxylic acid, COSY, NOESY, HSQC, HMBC, XRD

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