Spectroscopic characterization of single co-crystal of mefenamic acid and nicotinamide using supercritical CO2

Ye.A. Vaksler,D. Benedis,A.A. Dyshin, R.D. Oparin,N.T. Correia, F. Capet, S.V. Shishkina,M.G. Kiselev,A. Idrissi

Journal of Molecular Liquids（2021）

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摘要

•Single co-crystal (1:2) of mefenamic acid and nicotinamide is grown from scCO2.•Its structure is studied by SCXRD and reference PXRD and IR pattern are obtained.•Influences of temperature, components ratio and duration are studied.•Efficiency of modified CSS method is compared to RESS.

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关键词

Co-crystallization,Single crystal,Supercritical carbon dioxide,X-ray diffraction,Infrared spectroscopy

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