Synthesis and organogelating behaviour of urea- and Fmoc-containing diphenylalanine based hexaamide

Stanislav A. Petrov,Aleksei E. Machulkin,Rostislav A. Petrov,Alexander N. Tavtorkin,Galina N. Bondarenko,Sergey A. Legkov,Ilya E. Nifant'ev,Valentina D. Dolzhikova,Nikolay V. Zyk,Alexander G. Majouga,Elena K. Beloglazkina

Journal of Molecular Structure（2021）

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Abstract

•A new hexaamide organоgelator with urea moiety was synthesized.•The gels form in DCM, CDCl3, MeOH, EtOAc, MeCN, MeCN/H2O.•Gel morphologies differ in DCM and methanol.•Gelator molecules aggregate via N–H/O, hydrophobic and π-π-interaction.

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Key words

Gel,Organogelation,Polyamide,Scanning electron microscopy,Solid phase peptide synthesis

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