Acylhydrazone Based on 2- N -Tosylaminobenzaldehyde and Girard T Reagent: Synthesis, Structure, and Coordination Ability

L. D. Popov,S. I. Levchenkov,V. V. Lukov, K. B. Gishko,S. A. Borodkin, Y. P. Tupolova, O. I. Askalepova,V. G. Vlasenko, D. V. Spiridonova,V. A. Lazarenko,A. S. Burlov,I. N. Shcherbakov

RUSSIAN JOURNAL OF GENERAL CHEMISTRY（2021）

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摘要

The novel hydrazone, a condensation product of 2- N -tosylaminobenzaldehyde and Girard T reagent, as well as the Cu(II), Ni(II), Co(II) and Fe(III) complexes on its base were synthesized. The ligand structure and properties were studied with IR, UV, 1 H NMR spectroscopy, mass-spectrometry, and potentiometry method. Structure of nickel(II) complex was determined by X-ray diffraction analysis.

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关键词

hydrazones, complex compounds, X-ray diffraction analysis, quantum-chemical calculations, magnetochemistry, spectroscopy

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