Study of thermally induced phase transformations and microstructural changes in porous MoO3 nanostructures for the design of tribological additives

Materials Letters(2021)

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Abstract
•Thermal evolution of MoO3 nanostructures between 30 and 455 °C is reported.•Monoclinic MoO3 follows dehydration, and Mo4O11 appears at higher temperatures.•Amorphous matrix crystallizes and is partially reduced, forming the suboxide.•Thermal and chemical processes affect phase and microstructure behavior of MoO3.
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Key words
Porous MoO3,Thermal X-ray diffraction,Electron irradiation,Phase transformations,Crystallization process,Reduction process
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