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羟基咔咯镓(Ⅲ)的合成及荧光性质研究

Lei SHI,Yuqi FANG, Mengying ZHAN, Qiwen WU,Canbin WANG,Xiang LI,Wei YIN

Journal of Guangdong University of Education（2019）

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Abstract
以10-(4-羟基苯基)-5,15-二(2,3,4,5,6-五氟苯基)咔咯为母体,和GaCl3进行反应得到10-(4-羟基苯基)-5,15-二(2,3,4,5,6-五氟苯基)咔咯镓配合物,产率为80％.采用核磁共振氢谱、质谱、紫外可见光谱对化合物进行表征.通过测定两种化合物的稳态吸收光谱和稳态荧光光谱,研究它们的光谱性质.结果表明:在浓度相同时,引入金属镓能够显著增加咔咯的吸收强度和荧光量子产率.
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