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N-(4-二苯胺苯甲基)-甘氨酰丝氨酸甲酯的合成

Zhi-fen LI,Jun-ling WANG,Jun QIAO,Lin XU,Hai XIE

Chemical Reagents（2017）

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Abstract
主要以甘氨酸和4-二苯氨基苯甲醛为原料,通过还原氨化反应得到4-二苯胺-苯甲氨基乙酸,用叔丁氧羰基保护二级氨后,与丝氨酸甲酯脱水缩合生成N-(4-二苯胺苯甲基)-N-叔丁氧羰基-甘氨酰丝氨酸甲酯,脱去保护基后得到标题化合物.用1HNMR、13CNMR、IR、MASS、HRMS和HPLC对目标化合物的结构进行了表征.
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4-diphenylaminobenzaldehyde,glycine,serine
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