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旋光性N-Boc-氮杂环丁烷-2-羧酸的规模化合成

Qi ZHANG,Qiang FENG,Tao HAN,Bing HE,Kang SUN,Xiaoling ZHANG,Zhonghui LI

Chemical World（2018）

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Abstract
以γ-丁内酯为原料,经溴代、酯化、环化、拆分、氢化、保护、水解等反应,合成了旋光性N-Boc-氮杂环丁烷-2-羧酸,总收率达到43％,中间体和目标化合物的结构均经1H NMR,13C NMR,HRMS确证.
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