meso-四(4-溴代苯基)卟啉的合成及其光学性能
Chinese Journal of Synthetic Chemistry（2018）
Abstract
采用改进"Alder法",以吡咯和对溴苯甲醛为原料,合成了meso-四(4-溴代苯基)卟啉(TBPP),其结构和性能经UV-Vis,FL和IR表征.研究了硝基苯用量、溶剂用量、溶剂浓缩量、投料比η[n(对溴苯甲醛)/n(吡咯)]和反应时间对TBPP收率的影响.结果表明:在最佳反应条件[吡咯25 mmol,η=1.05/1,丙酸70 mL,硝基苯2 mL,溶剂浓缩量30 mL,回流反应40 min]下,TBPP收率30.68%.
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Key words
meso-tetra(4-bromophenyl)porphyrin,pyrrole,Alder's method,synthesis,optical property
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