微波快速合成2-氨甲基苯并咪唑
Speciality Petrochemicals（2008）
Abstract
将0.22 mol邻苯二胺和0.22 mol氨基乙酸溶于6 mol/L 100 mL盐酸中,用微波辐射7 h制备了2-氨甲基苯并咪唑,经后处理得到白色固体,熔点45～47℃,产率46.4%。利用FT-IR、~1H NMR对产物进行了结构表征。
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Key words
ortho-phenylenediamine,glycine,microwave radiation,2-aminomethylbenzimidazole
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