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血塞通中皂苷类成分的SPE-ESI-MS/MS分析

Nana ZHAO,Hui LIU,Daolei SUN,Xinhe LIANG,Hui ZHANG,Jiaming SUN

Jilin Journal of Traditional Chinese Medicine（2018）

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Abstract
目的 通过固相萃取-电喷雾串联质谱(SPE-ESI-MS/MS)法快速分析血塞通中三七总皂苷成分.方法 采用Agilent SampliQ C18固相萃取柱对血塞通中三七总皂苷成分进行纯化和分离,通过ESI-MS/MS分析鉴定其皂苷类成分.结果 鉴定了血塞通中三七总皂苷6种常见的皂苷类成分,为人参皂苷Rb1、Rc、Rd、Rg1、Rh1和三七皂苷R1.结论 本方法简便、可靠,为快速检测血塞通中有效成分三七总皂苷提供了有效方法,同时也为以三七总皂苷成分为原料的药品质量控制方法研究提供参考.
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Key words
Xuesaitong,Ginsenosides,SPE-ESI-MS/MS
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