顶空固相微萃取-气质联用法测定四磨汤口服液挥发性成分

Fei-ya LUO,Qi TANG,Miao-fen CHEN,Pi CHENG, Yi-cong ZHOU, Deng-tian CAO,Jian-guo ZENG,Hua YANG,Ya-jie ZHENG

Chinese Traditional Patent Medicine（2019）

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Abstract

目的采用顶空固相微萃取-气质联用HS-SPME-GC-MS法测定四磨汤口服液挥发性成分.方法通过HS-SPME-GC-MS检测四磨汤口服液及单味药材中挥发性成分;NIST.14谱库检索结合文献对其挥发性成分进行鉴定以及成分比较.结果从中鉴定了13种挥发性成分,它们的峰面积和占总峰面积的91.62％.其中芳樟醇、α-松油醇、(Z,Z,Z)-9,12,15-十八碳三烯-l-醇和百里香酚等存在单味药材中,反式芳樟醇氧化物(呋喃)、(-)香芹酮和顺式香叶醇是枳壳药材中特有的挥发性成分.结论该方法灵敏度高,能实现复杂中药体系的挥发性成分分析,为完善和提升中药复方制剂质控体系提供参考.

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