补正续骨泡腾颗粒质量标准研究
Journal of Liaoning University of Traditional Chinese Medicine（2017）
Abstract
目的:建立补正续骨泡腾颗粒的质量标准.方法:采用显微鉴别法对方中鹿茸进行显微定性鉴别,采用薄层色谱法对方中制何首乌、合欢花、骨碎补进行定性鉴别,采用高效液相色谱法测定续断中川续断皂苷Ⅵ含量.结果:薄层色谱斑点清晰,阴性液无干扰,显微特征明显,川续断皂苷Ⅵ在3.465～20.79μg范围内呈良好的线性关系(r=0.9999),平均回收率为99.8％.结论:该方法准确,专属性强,重复性好,可以作为控制补正续骨泡腾颗粒质量的方法.
MoreKey words
Buzheng Xugu Effervescent Granule,Polygoni Multiflori Radix Praeparata,Albiziae Flos,Drynariae Rhizoma,Cervi Cornu Degelatinatum,asperosaponin Ⅵ,microscopic identification method,TLC,HPLC
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