枳壳药材的指纹图谱研究
Guiding Journal of Traditional Chinese Medicine and Pharmacology(2016)
Abstract
目的:应用HPLC法对枳壳药材进行指纹图谱研究.方法:色谱条件:Thermo Syncronis-C18(250 mm×4.6 mm,5 μm),以乙腈-0.1%磷酸溶液为流动相进行梯度洗脱,柱温为30℃,检测波长为300 nm(0~24 min)和215 nm(24.01~70 min),流速为1 mL/min.结果:10批样品有12个共有峰,指纹图谱对枳壳中各成分均有较好分离.结论:该方法简便,准确,重复性好,能有效地对其质量进行评价.
MoreKey words
Zhike (Aurantii Fructus),HPLC,fingerprint
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