HPLC-DAD法研究注射用盐酸多柔比星含量测定方法
Strait Pharmaceutical Journal(2014)
Abstract
目的:建立新的注射用盐酸多柔比星含量测定的方法。方法采用HPLC-DAD方法,以0.05mol· L -1磷酸二氢钾溶液(用25%氢氧化钠溶液调节pH至7.5)∶乙腈(70∶30)为流动相,检测波长为247nm。结果盐酸表柔比星在1~1000mg· mL -1内呈良好的线性关系(r =0.9999),平均回收率为100.58%( n=9)。结论本方法简单通用,准确性好,可用于注射用盐酸表柔比星含量测定的检查。
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Key words
Epirubicin Hydrochloride for Injection,HPLC-DAD,Content determination
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