苗药蓝布正制剂云实感冒合剂中鞣花酸的含量测定
Journal of Traditional Chinese Veterinary Medicine(2018)
Abstract
目的:建立云实感冒合剂中的鞣花酸含量测定方法.方法:采用Agilent Technologies 1290 InfinityUHPLC进行测定,色谱柱为Phenomenex Synergi(2.0 mm×100 mm,2.5 μm),柱温为40℃,流动相为甲醇-0.1%甲酸溶液,梯度洗脱,流速为0.3 mL/min,检测波长为254 nm,进样量为3 μL.结果:经方法学考察,6批云实感冒合剂中的鞣花酸含量线性关系良好.结论:该方法操作简单、快速、准确和重复性好,可用于云实感冒合剂的质量控制.
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