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硫代酯抗氧剂412S的合成研究

Zhuo-hua TAN,Shi-chang LI,Xiao-juan AO,Yu-nong YANG,Hao-jiang WANG,Fei WANG,Zu-bi LEI

Synthetic Materials Aging and Application（2018）

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Abstract
季戊四醇四(3-月季基硫代丙酸酯)是一种耐热、耐水解性能优异的塑料抗氧剂,应用于各种聚烯烃和工程塑料中.本文以十二烯、3-巯基丙酸、季戊四醇等为主要原料,在偶氮化合物存在下制备季戊四醇四(3-月季基硫代丙酸酯).实验表明,当十二烯、3-巯基丙酸和季戊四醇的摩尔比为1.14:1:0.22时,制备的季戊四醇四(3-月季基硫代丙酸酯)收率可达90.7％.
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