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仲丁氨基甲酸甲酯的合成

Yufeng Yang,Zezhi Zhang

Speciality Petrochemicals（2018）

Cited 0|Views4
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Abstract
采用碘化钾催化仲丁胺与碳酸二甲酯的反应合成仲丁氨基甲酸甲酯.实验考察了仲丁胺与碳酸二甲酯的摩尔比、反应时间、催化剂及用量对反应的影响,结果表明:碘化钾催化活性高、易于分离;较佳的合成条件为n(仲丁胺):n(碳酸二甲酯)=1:3,反应时间9h,碘化钾的加入量0.8％.在此条件下产物收率大于79％,纯度大于98％.
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