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催化异构化合成挂式四氢双环戊二烯

Yong-mei DU,Chun-ying LI,Qiang SHI,Jian L(U)

INDUSTRIAL CATALYSIS（2005）

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Abstract
对催化异构化桥式四氢双环戊二烯合成挂式四氢双环戊二烯的反应进行了研究.考察了无水AlCl3催化下,溶剂、溶剂用量、催化剂用量和反应时间对转化率以及选择性的影响.结果表明,以CH2Cl2为溶剂,CH2Cl2和桥式四氢双环戊二烯的用量比为0.8,催化剂用量为20%,反应时间为3 h,桥式四氢双环戊二烯的转化率为97.12%,挂式四氢双环戊二烯的选择性为99.28%.
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Key words
catalytic isomerization,synthesis,exo-tetrahydrodicyclopentadiene
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