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Mo5SiB2-Based Ceramics by Forced SHS Compaction and Hot Pressing of SHS-Produced Powders: Features of Phase-Formation Processes

Potanin A. Yu.,Pogozhev Yu. S.,Rupasov S. I.,Novikov A. V.,Kovalev D. Yu.

INTERNATIONAL JOURNAL OF SELF-PROPAGATING HIGH-TEMPERATURE SYNTHESIS（2020）

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Abstract
Mo5SiB2-based ceramics were fabricated from elemental powders by forced SHS compaction and hot pressing of SHS-produced powders and specific features of product patterning were characterized by XRD, time-resolved XRD, SEM/EDS, and TEM/EDS. Best results were obtained upon hot pressing of SHS-produced Mo–Si–B powders: resultant material was single-phased Mo5SiB2 with a mean grain size of 2–10 μm.
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Key words
combustion synthesis,SHS,forced SHS compaction,hot pressing,Mo5SiB2,time-resolved XRD
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