General Method for Quantitation of Organic Hydroperoxides
ORGANIC PROCESS RESEARCH & DEVELOPMENT(2020)
Abstract
The utility of peroxides in synthetic organic chemistry is tied to significant safety risks posed by their handling, storage, and disposal. Although guidelines exist, a lack of reliable methods for quantitation of low levels of these species has been a major impediment to establishing data-driven safety guidelines and protocols. This paper discloses a general and reliable liquid chromatography-ultraviolet (LC-UV)-based method for the detection of a wide range of commonly encountered organic hydroperoxides. The implications of this method for safety concerns around trace peroxides are also discussed, supported by modern thermochemical analysis.
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Key words
peroxides,safety,oxidation,solvents
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