Synthesis and Crystal Structure of 4-Amino-3, 5-Dinitropyrazole Sodium Salt

Yinglei Wang,Yongfei Pan,Weixiao Liu,Yueping Ji,Fulei Gao,Feng Ding

AIP Conference Proceedings（2018）

Cited 4|Views10

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Abstract

A novel energetic material, 4-amino-3,5-dinitropyrazole sodium salt (ADNPNa), was firstly synthesized in a yield of 86.26%. The structure of ADNPNa Was confirmed by IR and elemental analysis. The single crystal of ADNPNa was determined by single crystal X-ray diffraction. The crystal belongs to triclinic system, space group P-1 with crystal parameters a=6.284(4)angstrom, b=6.480(4)angstrom, c=9.729(6)angstrom, beta= 95.294(9)degrees, V=365.0(4)angstrom(3), Z=2, mu=0.227mm(-1), F(000)= 216, and D-c=1.939g/cm(3).

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Key words

4-amino-3,5-dinitropyrazole sodium salt (ADNPNa),Crystal structure

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