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Hydrolytic polycondensation of trimethoxymethylsilane under ultrasonic irradiation

Nikita G. Yakhontov,Olga B. Gorbatsevich,Alexandra A. Kalinina,Nina V. Demchenko,Valentina V. Kazakova,Aziz M. Muzafarov

MENDELEEV COMMUNICATIONS（2020）

Cited 4|Views15
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Abstract
The hydrolytic polycondensation of trimethoxymethylsilane in the absence of catalyst and solvent under ultrasonic irradiation was performed, the effect of reagent ratio, power, temperature and irradiation duration on the process outcome was estimated. Thus obtained polyorganosilsesquioxanes were characterized by H-1 NMR and IR spectroscopy as well as gel permeation chromatography.
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Key words
hydrolytic polycondensation,alkoxysilanes,trimethoxymethylsilane,polyorganosilsesquioxanes,ultrasonic irradiation
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