Synthesis of 1,2-dihydro-1,3,5-triazine derivatives via Cu(II)-catalyzed C(sp 3 )-H activation of N , N -dimethylethanolamine with amidines.
CHEMICAL COMMUNICATIONS(2020)
摘要
1,2-Dihydro-1,3,5-triazines and symmetrical 1,3,5-triazines were obtained in up to 81% yields from amidines andN,N-dimethylethanolamine catalyzed by CuCl2. The reaction involves three C-N bond formations during the oxidative annulation process and the mechanism was proposed. This efficient synthesis of 1,2-dihydro-1,3,5-triazines was developed for the first time.
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