Development and validation of a combined enzymatic-digestion/mass spectrometry assay for Tacrolimus quantitation in cardiac biopsies.

Mariadelfina Molinaro,Carlo Pellegrini,Barbara Cattadori,Simona De Gregori

Journal of Chromatography B（2020）

引用 4|浏览13

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摘要

•A validated LC MS/MS assay for the quantitation of Tacrolimus in cardiac biopsies.•Optimization of samples preparation.•Method validation results in swine cardiac biopsies.•First applications to human endomyocardial tissue.

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关键词

Tacrolimus,Heart biopsy,Organ rejection,Enzymatic digestion,Mass spectrometry

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