Synthesis of 1,3-diaryl butanones from acetophenones via a tandem reaction
SYNTHETIC COMMUNICATIONS(2020)
摘要
A tandem reaction for the simple construction of 1,3-diaryl butanones from acetophenones was developed. Anhydrous HI was generated in situ by the promotion of the [Rh]- complex with molecular hydrogen and iodine. The acetophenones undergo aldol reactions by anhydrous HI firstly, and then hydrogenation reactions by the same [Rh]-complex to generate the corresponding 1,3-diaryl butanones in one pot.
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关键词
Acetophenones,aldol reaction,anhydrous HI,molecular hydrogen,molecular iodine
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