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Highly conjugative heterocyclic nitrogen base derivative and its metal complexes towards optoelectronic materials: Chemical architecture, synthesis, structural elucidation, catalytic, optoelectronic and pharmacological studies

Materials Today: Proceedings(2021)

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摘要
The pharmacologically active structural architecture of highly conjugative heterocyclic structure core comprised of 1, 10-Phenanthroline derivatives with different metal acetates to arrive different complexes with molecular formulae of [MIIL] where L = 1,10-Phenanthroline derivative. The structural features of synthesized compounds using elemental compositions, molar conductivity, magnetic properties as well spectral (UV–Vis., IR, NMR, ESR), thermal analysis and cyclic voltammetry protocols. On the basis of analytical and spectroscopic approaches demonstrated that an octahedral geometry for the Co(II), Zn(II), Cu(II) and Ni(II) chelates. The voltage–current output was utilized to conclude the threshold voltage (Von) of synthesized metal complexes as emerging materials. The catalytic conversion of benzyl alcohol into benzaldehyde and to optimize the reaction situations were performed to attain enhanced turn over number. The prepared title chelates were accessed for antibacterial efficiency with B. subtilis, E. coli, S. aureus,) and fungi strains (A. flavus, C. albicans and A. niger). The observed outcomes has indicated that the complexes showed greater antimicrobial efficiencies than ligand. Additionally, the SOD biomimetic activity of prepared metal complexes was measured and discussed. Antituberculosis efficiencies of 1,10-Phenanthroline derivative and its chelates was assessed against strain, M. tuberculosis H37Rv with the help of MABA assay protocol.
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关键词
Complexes,Catalytic,Voltage,Biomimetic,Antimicrobial
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