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In-situ observation of structural and chemical transitions in B4C based layered systems

Christian Morawe,Phakkhananan Pakawanit,Ratchadaporn Supruangnet,Narong Chanlek,Dechmongkhon Kaewsuwan,Jean-Christophe Peffen,Sylvain Labouré

Applied Surface Science（2020）

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Abstract
•Boron depletion in B4C based thin layered systems was investigated.•Pt/B4C was studied with in-situ X-ray reflectivity during annealing in air.•The study was complemented by depth-resolved XPS, EDX, and TEM.•An interplay of reactive B4C, catalytic Pt, and protective C was observed.•The method is a convenient tool to optimize multilayer fabrication strategies.
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Key words
X-ray multilayers,Multilayer degradation,In-situ X-ray reflectivity,Thermal annealing
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