Unprecedented yield of methyl-esterification with in-situ generated diazomethane in a microchannel reactor with methanol as solvent

Xuezhi Duan,Zikun Huang,Gang Qian,Kuan He,Jing Zhang,Leslaw Mleczko,Xinggui Zhou

Chemical Engineering Science（2020）

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摘要

•The methylesterfication of in-situ generated CH2N2 exhibits remarkable solvent effects.•The low ester yield mainly arises from its transesterification.•Unprecedented high ester yield is achieved using methanol as solvent.

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关键词

Microreaction technology,Methyl-esterfication,Diazomethane,Solvent effects,Transesterification

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