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Preparative enantioseparation of synephrine by conventional and pH-zone-refining counter-current chromatography.

Yang Zhang,Shanshan Wang,Jianguang Luo,Yaolan Lin, Xiao Xu,Chao Han,Lingyi Kong

Journal of Chromatography A（2018）

Cited 15|Views3
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Abstract
•Chiral CCC was superior to HPLC for preparative separation of synephrine.•pH-zone-refining CCC allowed efficient preparative enantioseparation of synephrine.•pH-zone-refining CCC was suited for preparative resolution of β-amino alcohols.
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Enantioseparation,High-speed counter-current chromatography,pH-zone-refining,Synephrine enantiomer,Di-n-hexyl L-tartrate
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