TRANSITION METAL CATALYZED OXIDATION, 10 : ZIRCONIUM-CATALYZED OXIDATION OF PRIMARY ALIPHATIC AMINES TO NITRO COMPOUNDS WITH TERT-BUTYL HYDROPEROXIDE

European Journal of Organic Chemistry（1998）

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摘要

Primary aliphatic amines are oxidized with tert-butyl hydroperoxide to the corresponding nitro compounds in 50-98% yield using Zr(Ot-Bu)(4) as the catalyst. The CH-acidic nitro compounds are not epimerized under these reaction conditions.

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关键词

aliphatic amines,aliphatic nitro compounds,oxidation,zirconium tetra-tert-butylate,tert-butyl hydroperoxide

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