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Synthesis and Crystal Structure of Dimorphic Dibenzo[cde,opq]rubicene.

Joghee R Suresh,Glenn Whitener,Gabriele Theumer,Dirk J Bröcher,Ingmar Bauer,Werner Massa,Hans-Joachim Knölker

CHEMISTRY-A EUROPEAN JOURNAL（2019）

Cited 7|Views48
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Abstract
Dibenzo[cde,opq]rubicene has been synthesized by an eight-step reaction sequence including an iron-mediated [2+2+1] cycloaddition and a flash vacuum pyrolysis as key steps. Two crystal modifications of the S-shaped, planar polycyclic aromatic hydrocarbon have been obtained and characterized by X-ray diffractometry.
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Key words
cycloadditions,flash vacuum pyrolysis,polycyclic aromatic hydrocarbons,polymorphism,X-ray diffraction
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