Metallomicelle catalyzed aerobic tandem desilylation/Glaser reaction in water

GREEN CHEMISTRY(2019)

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摘要
PEG-grafted nitrogen ligands were synthesized. The corresponding copper complexes serve as metallomicellar nanoreactors for the aerobic tandem desilylation/ Glaser coupling of TMS-protected alkynes in water. The protocol is also suitable for base-free homocoupling of terminal alkynes. The metallomicellar catalyst could be recycled 5 times with minor loss of reactivity.
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关键词
Metal-Free Hydrogen Activation,Nickel-Catalyzed
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