Rational synthesis of α-hydroxyphosphonic derivatives including dronic acids
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS（2019）
Abstract
New, green methods have been elaborated for the syntheses of -hydroxyphosphonates and -hydroxymethylenebisphosphonic derivatives (HMBPs, dronates). -Hydroxyphosphonates were prepared via the Pudovik reaction, while the synthesis of HMBPs has been performed in the three-component reaction of carboxylic acids, phosphorus trichloride and phosphorus acid. [GRAPHICS] .
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Key words
alpha-Hydroxymethylenebisphosphonates,-hydroxyphosphonates,Pudovik reaction,green syntheses,sulfolane,ionic liquid
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