Synthesis and Structural-Energy Characteristics of Fe-BDC Metal-Organic Frameworks

M. K. Knyazeva,A. V. Shkolin,A. A. Fomkin,A. Yu. Tsivadze,O. V. Solovtsova, N. P. Platonova,A. L. Pulin,I. E. Men’shchikov,A. A. Shiryaev,V. V. Vysotskii,M. R. Kiselev

Protection of Metals and Physical Chemistry of Surfaces（2019）

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摘要

A metal-organic framework, Fe-BDC, was synthesized by solvothermal method from iron salt and terephthalic acid using N , N -dimethylformamide as the solvent. The data from the study of structural-energy characteristics calculated by the Dubinin-Radushkevich, Kelvin, and BET equations are given. The resulting Fe-BDC sample has a specific surface area of S BET = 2240 m 2 /g and a specific micropore volume of W 0 = 0.83 cm 3 /g. The morphological and X-ray characteristics of this sample were studied.

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关键词

metal-organic framework,MOF,iron,BDC,adsorption,micropores,mesopores

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