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UV-induced catalyst-free intramolecular formal Heck reaction

Wangsheng Liu,Dongmei Ma,Hao Guo,Guangxin Gu

Journal of Saudi Chemical Society（2019）

Cited 7|Views4
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Abstract
A catalyst-free intramolecular formal Heck reaction has been developed, affording 9-benzylidene-9H-fluorene derivatives under UV irradiation. This reaction probably proceeds via UV-induced homolytic cleavage of CI bond, addition of the aryl radical to the alkene moiety, single electron oxidation of alkyl radical intermediate into carbocation species, and deprotonation.
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Key words
Photochemistry,Cyclization,Radical,Fluorene
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