An Unprecedented {Ni14siw9} Hybrid Polyoxometalate With High Photocatalytic Hydrogen Evolution Activity

Gregoire Paille,Amandine Boulmier, Alexandre Bensaid,Minh-Huong Ha-Thi,Thu-Trang Tran,Thomas Pino,Jerome Marrot,Eric Riviere,Christopher H. Hendon,Olivier Oms,Maria Gomez-Mingot,Marc Fontecave,Caroline Mellot-Draznieks,Anne Dolbecq,Pierre Mialane

CHEMICAL COMMUNICATIONS（2019）

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摘要

A unique polyoxometalate complex made up of a tetradecanuclear nickel bisphosphonate cluster capping a {SiW9} unit has been characterized. This stable compound exhibits a high hydrogen evolution reaction photocatalytic activity under visible light irradiation via a reductive quenching mechanism.

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