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Step by step and one-pot syntheses of 5-hydroxy-5-(polyfluoroalkyl)isoxazol-4(5 H )-one oximes

Nadezhda V. Palysaeva,Nadezhda S. Boltacheva,P. A. Slepukhin,M. G. Pervova,V. I. Filyakova,Aleksei B. Sheremetev,Valery N. Charushin

Mendeleev Communications（2018）

Cited 8|Views13
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Abstract
5-Hydroxy-5-(polyfluoroalkyl)isoxazol-4(5H)-one oximes have been obtained by nitrosation of lithium 3-polyfluoroalkyl-1,3-diketonates followed by treatment of intermediate 3-(poly-fluoroalkyl)propane-1,2,3-trione 2-oximes with hydroxylamine hydrochloride. The one-pot protocol comprising both stages has been elaborated.
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oximes,syntheses,one-pot
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