Effect of the thermal treatment on the magnetic and structural properties of cobalt ferrite particles
Ceramics International(2016)
Abstract
We herein report a study on the sol-gel synthesis of CoFe2O4 and the effect of thermal treatment on the product outcome. Xerogels treated at 750, 800 and 850°C had their structural and magnetic properties thoroughly studied, in order to correlate their synthesis conditions to the positions in which the cations are inserted in the spinel structure. X-ray diffractograms exhibit reflections representative of the spinel structure and demonstrate that the thermal treatment does not affect the lattice parameters of the material. Mossbauer spectroscopy studies indicate a very low inversion degree in the synthesized spinels, which is very unusual for CoFe2O4. A maximum in coercivity of 1405.2 Oersted was achieved for the sample treated at 800°C.
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Key words
Sol-gel processing,Magnetic properties,Ferrites,Spinels
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