对硝基苯甲醛缩对羟基苯甲酰腙的合成与晶体结构
Chemical Research(2010)
Abstract
合成了一种新的对硝基苯甲醛缩对羟基苯甲酰腙晶体;利用红外光谱、紫外光谱和元素分析对其进行了表征,并利用单晶X射线衍射测定了其晶体结构. 结果表明,该晶体属于单斜晶系,P2(1)/n空间群;晶胞参数a = 0.766 17(2)nm,b = 1.357 3(3)nm,c = 1.256 0(3)nm,β = 92.71(3)°,V = 1.304 7(4)nm3,Z = 4,Dc = 1.452 g/cm3,μ = 0.109 mm-1. 12 593个可观察独立衍射点(I > 2σ(I))偏离因子R1= 0.042 5, wR2 = 0.142 4, S =1.096.
MoreTranslated text
Key words
p-hydroxybenzalhydrazone,crystal structure,p-nitrobenzaldehyde,synthesis
AI Read Science
Must-Reading Tree
Example
![](https://originalfileserver.aminer.cn/sys/aminer/pubs/mrt_preview.jpeg)
Generate MRT to find the research sequence of this paper
Chat Paper
Summary is being generated by the instructions you defined