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EFFICIENT MICROWAVE-ASSISTED SYNTHESES OF A SERIES OF NOVEL MONO(IMINO)PYRROLYL COMPOUNDS

Biyun Su,Xiaoteng Li, Xudong Wang

HETEROCYCLES（2015）

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Abstract
A series of novel mono(imino)pyrroles that were hard to prepare under traditional solvent reaction condition were readily synthesized under solvent free condition using microwave chemistry via p-TSA (p-toluenesulfonic acid) catalyzed Schiff base condensation. The structures of the compounds were characterized by means of MS, H-1 NMR, IR, elementary analysis and X-ray diffraction analysis. The reactivity of different aromatic amines with 2-acetylpyrrole was discussed.
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Mono(imino)pyrrole,Microwave Chemistry,Crystal Structure
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