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Radical Metalloids with N-Heterocyclic Carbene and Phenanthroline Ligands: Synthesis, Properties, and Cross-Coupling Reaction of [(Nitronyl Nitroxide)-2-ido]metal Complexes with Aryl Halides

Kiyomi Yamada,Xun Zhang,Ryu Tanimoto,Shuichi Suzuki,Masatoshi Kozaki,Rika Tanaka,Keiji Okada

BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN（2018）

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Abstract
New radical metalloids, NN-AuSIMes and NN-Cu(bdmpphen), were prepared and their properties were investigated. They were applied to Pd(0)-mediated crosscoupling reactions with aryl halides (ArX) to produce 2-aryl (nitronyl nitroxide)s in moderate to high yields.
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Key words
Radical metalloid,N-Heterocyclic carbene,Cross-coupling reaction
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