Synthesis and structure of 2-substituted pyrene-derived scaffolds
Tetrahedron Letters（2017）
Abstract
•We report the optimised synthesis of key 2-functionalized pyrene building blocks.•The compounds may be used as tags in the preparation of fluorescent probes.•Crystal structures of tetrahydropyrene and 2-acetyl-tetrahydropyrene are disclosed.•We report the crystal structure of ethyl tetrahydro-2-pyrene-5-oxopentanoate (ETPO).•ETPO is a key block for access to ester- or amide-bridged fluorescent probes.
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Key words
2-Functionalized pyrenes,Tetrahydropyrene,Ethyl 4,5,9,10-tetrahydro-2-pyrene-5-oxopentanoate,2-Acetyl-4,5,9,10-tetrahydropyrene
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