Traceless Linking of Indoles: General Methodology and Application to Solid Phase Supported Mannich and Stille Reactions

Johannes Kraxner, Michael Arlt,Peter Gmeiner

SYNLETT（2000）

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摘要

Transacetalization reaction of the diethoxymethyl (DEM) protected indoles 2a,b,d,e with the polymer bound glycerol derivative 3 resulted in formation of the immobilized indoles 4a,b,d,e. Selective indole-functionalizations as well as quantitative and traceless cleavage could be demonstrated.

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关键词

solid-phase synthesis,traceless linker,indoles,Stille reaction,diethoxymethyl protection

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