Trace level determination of chloroacetyl chloride and degradation products by derivatization gas chromatography.

Marie-France Morissette,Larry Wigman, Jerry Tso

Journal of Pharmaceutical and Biomedical Analysis（2018）

引用 3|浏览7

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摘要

•Simple GC-FID derivatization method for determination of chloroacetyl chloride.•Simultaneously monitored two degradation products using same analytical conditions.•Optimized derivatization conditions for maximum yields and reaction times.•Validated analytical method for different pharmaceutical matrices.

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关键词

Chloroacetyl chloride,Impurities,GC-FID,Derivatization,Traces analysis

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