A concise synthesis of substituted benzoates

Ashley D. Carbaugh, Wesley Vosburg,Tamara J. Scherer, Christopher E. Castillo, Matthew A. Christianson, Jennifer Kostarellas, Sager J. Gosai,Michael S. Leonard

ARKIVOC（2007）

Cited 13|Views15

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Abstract

Cycloaromatization, via tandem cycloaddition – extrusion of carbon dioxide, between methyl isodehydroacetate or methyl coumalate and a variety of alkyne dienophiles has been investigated. This method provides an efficient synthesis of methyl 4-hydroxymethyl-2,6dimethylbenzoate (1), a key intermediate in the preparation of retinal-based molecular probes.

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