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A facile method for the synthesis of indole phytoalexin rutalexin

Mariana Budovska,Zuzana Kudlickova,Peter Kutschy,Martina Pilatova,Jan Mojžis

Tetrahedron Letters（2015）

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Abstract
Novel methods for the preparation of the indole phytoalexin rutalexin (8) in high yields are presented. The synthesis of rutalexin (8) was achieved from previously synthesized 9-tert-butoxycarbonyl-2-methoxy-4-oxo-[1,3]thiazino[6,5-b]indole (5) by its hydrolysis, methylation, and deprotection. A second method starting from 9-Boc-cyclobrassinin (9) involved oxidation, methylation, and deprotection.
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Key words
Indoles,Phytoalexins,Rutalexin,Natural products
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