Solvent-free synthesis of 2-aminothiophene-3-carbonitrile derivatives using high-speed vibration milling
Journal of Chemical Research-s(2014)
Abstract
The solvent-free synthesis of 2-aminothiophene-3-carbonitrile derivatives by high-speed vibration milling using the inexpensive and environmentally friendly Et2NH as a catalyst was studied. The reaction conditions were optimised and the derivatives were obtained in good yield. This method has advantages in terms of short reaction time and facile conditions.
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Key words
solvent-free synthesis,high-speed vibration milling,2-aminothiophene
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