Group 8 Metallomacrocycles - Synthesis, Characterization, And Stability
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY（2015）
摘要
The one-step synthesis of the first homoleptic metallomacrocycle is reported. Characterization of the Os-II complex, along with its Fe-II and Ru-II analogues, was accomplished by NMR spectroscopy, ESI-MS, TWIM-MS, gradient tandem-MS, CV, luminescence and UV/Vis spectroscopy. Center-of-mass collision energies, derived from gradient tandem-MS, reveal that the -based structures are more stable than those of .
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关键词
Supramolecular chemistry,Self-assembly,Metallocycles,Osmium
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